Data provided by National Institute of Standards and Technology
This data set contains the instrument files (.pssession) as well as the extracted voltammogram data as (.xlsx) for voltammetric analysis of lead, diphenylamine, ferrocyanide, naltrexone, and acetaminophen collected during the generation of calibration curves and serial dilutions. Ferrocyanide data was collected via cyclic voltammetry between -300 mV and +700 mV with a scan rate of 100 mV/s and a potential sweep of 2 mV. Lead and diphenylamine data was collected via square-wave anodic stripping voltammetry with a deposition potential of -950 mV for 120 s and then swept from -1000 mV to + 1200 mV with a potential step of 5 mV, amplitude of 25 mV, and frequency of 11 Hz. Naltrexone data was collected via square-wave voltammetry between -1000 mV and +1200 mV with a potential step of 15 mV, amplitude of 100 mV, and a frequency of 100 Hz. Acetaminophen data was collected via square-wave voltammetry for the anodic direction between -600 mV and +1000 mV and the cathodic direction from +1000 mV to -600 mV both with a potential step of 4 mV, amplitude of 250 mV, and a frequency of 75 Hz.
About this Dataset
Updated: 2025-04-06
Metadata Last Updated:
2024-06-26 00:00:00
Date Created:
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Data Provided by:
Dataset Owner:
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| Title | Voltammogram Data Associated with Manuscript titled: "Strategies for Assessing the Limit of Detection in Voltammetric Methods: Comparison and Evaluation of Approaches." |
|---|---|
| Description | This data set contains the instrument files (.pssession) as well as the extracted voltammogram data as (.xlsx) for voltammetric analysis of lead, diphenylamine, ferrocyanide, naltrexone, and acetaminophen collected during the generation of calibration curves and serial dilutions. Ferrocyanide data was collected via cyclic voltammetry between -300 mV and +700 mV with a scan rate of 100 mV/s and a potential sweep of 2 mV. Lead and diphenylamine data was collected via square-wave anodic stripping voltammetry with a deposition potential of -950 mV for 120 s and then swept from -1000 mV to + 1200 mV with a potential step of 5 mV, amplitude of 25 mV, and frequency of 11 Hz. Naltrexone data was collected via square-wave voltammetry between -1000 mV and +1200 mV with a potential step of 15 mV, amplitude of 100 mV, and a frequency of 100 Hz. Acetaminophen data was collected via square-wave voltammetry for the anodic direction between -600 mV and +1000 mV and the cathodic direction from +1000 mV to -600 mV both with a potential step of 4 mV, amplitude of 250 mV, and a frequency of 75 Hz. |
| Modified | 2024-06-26 00:00:00 |
| Publisher Name | National Institute of Standards and Technology |
| Contact | mailto:[email protected] |
| Keywords | voltammetry , square-wave , cyclic voltammetry , electrochemistry , limit of detection , performance measures , validation parameters , forensic science , forensic chemistry |
{
"identifier": "ark:\/88434\/mds2-3388",
"accessLevel": "public",
"contactPoint": {
"hasEmail": "mailto:[email protected]",
"fn": "Colby Ott"
},
"programCode": [
"006:045"
],
"landingPage": "https:\/\/data.nist.gov\/od\/id\/mds2-3388",
"title": "Voltammogram Data Associated with Manuscript titled: \"Strategies for Assessing the Limit of Detection in Voltammetric Methods: Comparison and Evaluation of Approaches.\"",
"description": "This data set contains the instrument files (.pssession) as well as the extracted voltammogram data as (.xlsx) for voltammetric analysis of lead, diphenylamine, ferrocyanide, naltrexone, and acetaminophen collected during the generation of calibration curves and serial dilutions. Ferrocyanide data was collected via cyclic voltammetry between -300 mV and +700 mV with a scan rate of 100 mV\/s and a potential sweep of 2 mV. Lead and diphenylamine data was collected via square-wave anodic stripping voltammetry with a deposition potential of -950 mV for 120 s and then swept from -1000 mV to + 1200 mV with a potential step of 5 mV, amplitude of 25 mV, and frequency of 11 Hz. Naltrexone data was collected via square-wave voltammetry between -1000 mV and +1200 mV with a potential step of 15 mV, amplitude of 100 mV, and a frequency of 100 Hz. Acetaminophen data was collected via square-wave voltammetry for the anodic direction between -600 mV and +1000 mV and the cathodic direction from +1000 mV to -600 mV both with a potential step of 4 mV, amplitude of 250 mV, and a frequency of 75 Hz.",
"language": [
"en"
],
"distribution": [
{
"downloadURL": "https:\/\/data.nist.gov\/od\/ds\/mds2-3388\/Acetaminophen%20Data.pssession",
"format": ".pssession",
"description": "Acetaminophen Data .pssession",
"mediaType": "application\/octet-stream",
"title": "Acetaminophen Data .pssession"
},
{
"downloadURL": "https:\/\/data.nist.gov\/od\/ds\/mds2-3388\/Acetaminophen%20Data.xlsx",
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{
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"mediaType": "application\/octet-stream",
"title": "Ferrocyanide Data .pssession"
},
{
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"format": ".xlsx",
"description": "Ferrocyanide Data .xlsx",
"mediaType": "application\/vnd.openxmlformats-officedocument.spreadsheetml.sheet",
"title": "Ferrocyanide Data .xlsx"
},
{
"downloadURL": "https:\/\/data.nist.gov\/od\/ds\/mds2-3388\/Lead%20and%20Diphenylamine%20Data.pssession",
"format": ".pssession",
"description": "Lead and Diphenylamine Data .pssession",
"mediaType": "application\/octet-stream",
"title": "Lead and Diphenylamine Data .pssession"
},
{
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"format": ".xlsx",
"description": "Lead and Diphenylamine Data .xlsx",
"mediaType": "application\/vnd.openxmlformats-officedocument.spreadsheetml.sheet",
"title": "Lead and Diphenylamine Data .xlsx"
},
{
"downloadURL": "https:\/\/data.nist.gov\/od\/ds\/mds2-3388\/Naltrexone%20Data.pssession",
"format": ".pssession",
"description": "Naltrexone Data .pssession",
"mediaType": "application\/octet-stream",
"title": "Naltrexone Data .pssession"
},
{
"downloadURL": "https:\/\/data.nist.gov\/od\/ds\/mds2-3388\/Naltrexone%20Data.xlsx",
"format": ".xlsx",
"description": "Naltrexone Data .xlsx",
"mediaType": "application\/vnd.openxmlformats-officedocument.spreadsheetml.sheet",
"title": "Naltrexone Data .xlsx"
}
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"bureauCode": [
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"modified": "2024-06-26 00:00:00",
"publisher": {
"@type": "org:Organization",
"name": "National Institute of Standards and Technology"
},
"theme": [
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"Forensics:Trace evidence",
"Forensics:Drugs and toxicology"
],
"keyword": [
"voltammetry",
"square-wave",
"cyclic voltammetry",
"electrochemistry",
"limit of detection",
"performance measures",
"validation parameters",
"forensic science",
"forensic chemistry"
]
}
