SRM 2969 Electronic files containing certified values and their uncertainties, and the data used to assign those values

Electronic files containing certified values and their uncertainties, and the data used to assign those values.

Here we provide curated analytical chemistry data for eggs collected from 1999 to 2010 on a subset of species and analytes that were measured regularly and reasonably systematically. Included in this publication are 487 samples analyzed for 174 ubiquitous environmental contaminants such as (poly)brominated diphenyl ethers (BDEs), mercury, organochlorine pesticides (OCPs), and polychlorinated biphenyls (PCBs). Data were collated to form a dataset useful in chemometric and related analyses of the marine ecosystem in the north Pacific Ocean.

These LC-MS and LC-MS/MS raw data were collected for purposes of an interlaboratory study evaluating the multi-attribute method (MAM). Tryptic digests of native NISTmAb (the "Reference" and the "Unknown" samples), degraded NISTmAb (the "pH Stress" sample) and NISTmAb spiked with 15 heavy-labeled synthetic peptides (the "Spike" sample) were sent to each participating laboratory. One injection of each digest was acquired in MS-only mode, while a second injection was acquired in MS/MS mode.

This tutorial provides mechanical drawings, electrical schematics, parts lists, STL files for 3D-printed parts, IGS files, and instructions for automated machining necessary for construction of a dual-protease, subzero, liquid chromatography system for hydrogen-deuterium exchange mass spectrometry. Electrical schematics for construction of a multi-zone temperature controller that regulate to ±0.1 oC are also included in this tutorial.

The project that produced these data involved the analysis and modeling of atmospheric Asian dust particles and background marine air particles collected in Hawaii, USA at the Mauna Loa Observatory (MLO) of the National Oceanic and Atmospheric Administration. Individual heterogeneous dust particles were analyzed with focused ion-beam scanning electron microscopy and energy-dispersive X-ray spectroscopy.

Data for mass concentration analysis and spectral analysis for the paper titled, "Comparison of primary laser spectroscopy and mass spectrometry methods for measuring mass concentration of gaseous elemental mercury"

Supporting datasets and algorithms (R-based) for the manuscript entitled "Development of a Tool to Determine the Variability of Consensus Mass Spectra", including an R Markdown script to reproduce the manuscript's figures.

SRM 3672 Organic Contaminants in Smokers' Urine (Frozen) - This Standard Reference Material (SRM) is intended for use in evaluating analytical methods for the determination of selected hydroxylated polycyclic aromatic hydrocarbons (hydroxylated PAHs) and phthalate, phenol, and volatile organic compound (VOC) metabolites in urine. All of the constituents for which certified and reference values are provided are naturally present in the urine. This data is public in the Certificate of Analysis for this material.

SRM 3673 Organic Contaminants in Non-Smokers' Urine (Frozen) - This Standard Reference Material (SRM) is intended for use in evaluating analytical methods for the determination of selected hydroxylated polycyclic aromatic hydrocarbons (hydroxylated PAHs) and phthalate, phenol, and volatile organic compound (VOC) metabolites in urine. All of the constituents for which certified and reference values are provided are naturally present in the urine. This data is public in the Certificate of Analysis for this material.