These four data files contain datasets from an interlaboratory comparison that characterized a polydisperse five-population bead dispersion in water. A more detailed version of this description is available in the ReadMe file (PdP-ILC_datasets_ReadMe_v1.txt), which also includes definitions of abbreviations used in the data files. Paired samples were evaluated, so the datasets are organized as pairs associated with a randomly assigned laboratory number.

These LC-MS and LC-MS/MS raw data were collected for purposes of an interlaboratory study evaluating the multi-attribute method (MAM). Tryptic digests of native NISTmAb (the "Reference" and the "Unknown" samples), degraded NISTmAb (the "pH Stress" sample) and NISTmAb spiked with 15 heavy-labeled synthetic peptides (the "Spike" sample) were sent to each participating laboratory. One injection of each digest was acquired in MS-only mode, while a second injection was acquired in MS/MS mode.

This tutorial provides mechanical drawings, electrical schematics, parts lists, STL files for 3D-printed parts, IGS files, and instructions for automated machining necessary for construction of a dual-protease, subzero, liquid chromatography system for hydrogen-deuterium exchange mass spectrometry. Electrical schematics for construction of a multi-zone temperature controller that regulate to ±0.1 oC are also included in this tutorial.

This is a file containing aggregation data for two proteins that were thermomechanically aggregated. The aggregated proteins were separated by asymmetric flow field flow fractionation and separated protein fractions were detected and quantified by UV spectrophotometry and multi-angle light scattering. The UV spectrophotometry was used to quantify the amount of residual monomer, which is reported herein. The multi-angle light scattering was fitted to a relevant model to calculate the molecular weight of the aggregated protein, also reported herein.

Supporting datasets and algorithms (R-based) for the manuscript entitled "Development of a Tool to Determine the Variability of Consensus Mass Spectra", including an R Markdown script to reproduce the manuscript's figures.

This Standard Reference Material (SRM) is intended for use as a primary calibration standard for the quantitative determination of tungsten. A unit of SRM 3163 consists of 50 mL of an acidified aqueous solution prepared gravimetrically to contain a known mass fraction of tungsten in a high-density polyethylene bottle sealed in an aluminized bag.

SRM 3669 Arsenic Species in Frozen Human Urine (Elevated Levels) - This Standard Reference Material (SRM) is intended primarily for validating analytical methods and measurements for the determination of arsenic species in human urine. A unit of SRM 3669 consists of five pouches each containing a vial of arsenic species in frozen human urine at elevated levels. Each vial contains nominally 1.5 mL of urine. This data is public in the Certificate of Analysis for this material.

Standard Reference Material 3949 Folate Vitamers in Frozen Human Serum

Standard Reference Material 909c Frozen Human Serum - This Standard Reference Material (SRM) is intended primarily for use in validating analytical methods for the determination of specified constituents in human serum. This SRM can also be used for quality assurance when assigning values to in house control materials. A unit of SRM 909c consists of three vials, each containing 2 mL of frozen human serum. This data is public in the Certificate of Analysis for this material.

Standard Reference Material (SRM) 968 and its reissues are human serum based materials used as validation standards by clinical, epidemiological, and nutrition laboratories. Historically, about 300 units of this SRM have been sold annually. Based on this annual sales projection, as of November 1, 2015 there were about 16 months of inventory of the current issue: SRM 968e Fat-Soluble Vitamins, Carotenoids, and Cholesterol in Human Serum.