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49 results found

Construction of a Dual-enzyme, Subzero (-30 degree C) Chromatography System and Multi-channel Precision Temperature Controller for Hydrogen-Deuterium Exchange Mass Spectrometry

Data provided by  National Institute of Standards and Technology

This tutorial provides mechanical drawings, electrical schematics, parts lists, STL files for 3D-printed parts, IGS files, and instructions for automated machining necessary for construction of a dual-protease, subzero, liquid chromatography system for hydrogen-deuterium exchange mass spectrometry. Electrical schematics for construction of a multi-zone temperature controller that regulate to ±0.1 oC are also included in this tutorial.

Tags: liquid chromatography,hydrogen-deuterium exchange,mass spectrometry,precision,peptide,protein,proteolysis,proteomics,reference material,temperature control.,

Modified: 2024-02-22

Views: 0

Calculation Sheet for Quasi-Static Position Calibration of the Galvanometer Scanner on the Additive Manufacturing Metrology Testbed

Data provided by  National Institute of Standards and Technology

This dataset includes a Microsoft Excel spreadsheet (*.xlsx file) provided as supplemental material for the NIST Technical Note (TN-2099) publication titled "Quasi-Static Position Calibration of the Galvanometer Scanner on the Additive Manufacturing Metrology Testbed". The file contains two tabs, titled "Pre-Compensation" and "Post-Compensation", which provides example measurement data and calculations pertaining to the calibration procedures described in the publication.

Tags: additive manufacturing,calibration,Galvanometer,Laser Powder Bed Fusion,

Modified: 2024-02-22

Views: 0

Supplementary Data for the paper "Three-Dimensional Particle Shape Analysis Using X-ray Computed Tomography: Experimental Procedure and Analysis Algorithms for Metal Powders" by E.J. Garboczi and N. Hrabe

Data provided by  National Institute of Standards and Technology

Supplementary Data for the paper "Three-Dimensional Particle Shape Analysis Using X-ray Computed Tomography: Experimental Procedure and Analysis Algorithms for Metal Powders" by E.J. Garboczi and N. Hrabe. Contains all the data and programs described in this paper to generate the results discussed in the paper. Also contains all the results that are generated by the data and programs, with which the user can compare to check their results.

Tags: additive manufacturing,metal powder,Laser Powder Bed Fusion,particle shape analysis,X-ray computed tomography. spherical harmonics,image analysis,powder analysis,powder particles,titanium alloy,Ti64,

Modified: 2024-02-22

Views: 0

Development of a Tool to Determine the Variability of Consensus Mass Spectra Supporting Data

Data provided by  National Institute of Standards and Technology

Supporting datasets and algorithms (R-based) for the manuscript entitled "Development of a Tool to Determine the Variability of Consensus Mass Spectra", including an R Markdown script to reproduce the manuscript's figures.

Tags: mass spectrometry,uncertainty analysis,per- and polyfluoroalkyl substances,PFAS,reference mass spectrum,

Modified: 2024-02-22

Views: 0

Thermographic measurements of single and multiple scan tracks on nickel alloy 625 substrates with and without a powder layer in a commercial laser powder bed fusion process (an additive manufacturing technology)

Data provided by  National Institute of Standards and Technology

This dataset contains thermographic measurements acquired during single and multiple track scans on bare substrates and on single layers of powder. The substrates and powder are nickel alloy 625 and the experiments are performed inside a commercial laser powder bed fusion machine. There are four experiment cases: 1) a single scan track on a bare substrate, 2) a single scan track on a single hand-spread layer of powder, 3) multiple (39) scan tracks covering an area on a bare substrate, and 4) multiple (39) scan tracks solidifying a single hand-spread layer of powder.

Tags: additive manufacturing,powder bed fusion,laser,thermography,temperature measurement,melt pool,melt pool length,cooling rate,Inconel 625,IN 625,nickel alloy 625,model validation,

Modified: 2024-02-22

Views: 0

Additive Manufacturing Benchmark Test Series (AM-Bench) 2018 Test Descriptions

Data provided by  National Institute of Standards and Technology

The Additive Manufacturing Benchmark Test Series (AM-Bench) is developing a continuing series of controlled benchmark tests, in conjunction with a conference series, with two initial goals: 1) to allow modelers to test their simulations against rigorous, highly controlled additive manufacturing benchmark test data, and 2) to encourage additive manufacturing practitioners to develop novel mitigation strategies for challenging build scenarios.

Tags: Additive Manufacturing Benchmark Test Series (AM-Bench),additive manufacturing,model validation,nickel alloy 625,15-5 Stainless Steel,In Situ Measurements,Residual Stress,Distortion,microstructure,Laser Powder Bed Fusion,melt pool,

Modified: 2024-02-22

Views: 0

In Situ Thermography of Single Scan Tracks Performed on Nickel Super Alloy 625 for the 2018 Additive Manufacturing Benchmark Test Series (AM-Bench 2018): Powder Bed Fusion Commercial Build Machine

Data provided by  National Institute of Standards and Technology

These measurements were performed as part of the 2018 Additive Manufacturing Benchmark Test Series (AM-Bench), specifically supporting the melt pool geometry challenge (CHAL-AMB2018-02-MP) and cooling rate challenge (CHAL-AMB2018-02-CR).

Tags: additive manufacturing,benchmark tests,AMBench,AMBench 2018,powder bed fusion,nickel super alloy 625,IN625,thermography,temperature measurement,melt pool length,cooling rate,

Modified: 2024-02-22

Views: 0

In situ thermography of the metal bridge structures fabricated for the 2018 Additive Manufacturing Benchmark Test Series (AM-Bench 2018)

Data provided by  National Institute of Standards and Technology

These measurements were performed as part of the 2018 Additive Manufacturing Benchmark Test Series (AM-Bench). This dataset and the associated experiments are part of a continuing series of controlled benchmark tests, in conjunction with a conference series, with two initial goals, 1) to allow modelers of Additive Manufacturing processes to test their simulations against rigorous, highly controlled additive manufacturing benchmark test data, and 2) to encourage additive manufacturing practitioners to develop novel mitigation strategies for challenging build scenarios.

Tags: additive manufacturing,benchmark tests,AMBench,AMBench 2018,powder bed fusion,nickel super alloy 625,IN625,thermography,cooling rate,temperature,

Modified: 2024-02-22

Views: 0

Hydrogen-Deuterium Exchange Mass Spectrometry (HDX-MS) Centroid Data measured between 3.6 degrees C and 25.4 degrees C for the Fab Fragment of NISTmAb

Data provided by  National Institute of Standards and Technology

The spreadsheet file reported herein provides centroid data, descriptive of deuterium uptake, for the Fab Fragment of NISTmAb (PDB: 5K8A) reference material, as measured by the bottom-up hydrogen-deuterium exchange mass spectrometry (HDX-MS) method. The protein sample was incubated in deuterium-rich solutions under uniform pH and salt concentrations between 3.6 degrees C and 25.4 degrees C for seven intervals ranging (0 to 14,400) s plus a control sample that simulates a Fab Fragment immersed for infinite time in D2O.

Tags: hydrogen-deuterium exchange,hydrogen exchange,HDX-MS,interlaboratory comparison,mass spectrometry,peptide,precision,proteomics,reference material,repeatability,reproducibility,

Modified: 2024-02-22

Views: 0

Variation of Surface Topography in Laser Powder Bed Fusion Additive Manufacturing of Nickel Super Alloy 625

Data provided by  National Institute of Standards and Technology

This dataset provides surface height data from nickel super alloy 625 experiment samples built through laser powder bed fusion additive manufacturing. The experiment methodically varied part position and orientation relative to the build plate and recoater blade and details of the experiment and dataset are available in a Journal of Research at NIST article.

Tags: additive manufacturing,focus variation,IN625,Laser Powder Bed Fusion,nickel super alloy 625,surface texture,surface topography,

Modified: 2024-02-22

Views: 0