The development of large residual elastic strains and stresses during laser powder-bed fusion (LPBF) additive manufacturing is one of the most significant barriers to widespread adoption. Accurate modeling of these strains and stresses is broadly recognized as an effective tool for mitigating these challenges, but rigorous validation data are needed. This data publication includes measurement data from diffraction-based characterizations of residual elastic strains in as-built (not heat treated) artifacts manufactured as part the the 2018 Additive Manufacturing Benchmark Series (AM Bench).

This repository contains two types of datasets: 4D-STEM data collected from a thermal annealing series of P3MEEMT films. 4D-STEM data:Dose series: Collected from P3MEEMT film annealed at 115 C. Each HDF5 file was generated from the raw data using the fpdpy software package to reshape and embed metadata. No other preprocessing was performed. Annealing series: Collected from P3MEEMT films annealed at 75 C, 115 C, 145 C, and 175 C. Each temperature contains two sets of 4D-STEM data collected at low and high magnification.

This data repository provides a central location for a body of work using one build of nickel-based alloy 718 (IN718) material and resulted in three different studies. The IN718 parts were manufactured by laser powder bed fusion using a range of laser energy densities (manipulation of processing variables) and orientations with respect to the build direction. The influence of processing variables on resulting grain structures, pore structures, and mechanical properties were studied in the as-built (not heat treated) condition.

This data set contains files included in the detailed instructional demonstration paper submitted to Integrating Materials and Manufacturing Innovation. The detailed instructional demonstration paper includes documentation detailing how to configure and carry out a repeatable Rietveld Refinement with the software MAUD. The data set provides: diffraction data from two different neutron diffraction measurements, crystallographic information files, and configuration files for the refinement process.

The absolute laser absorption was measured simultaneously with X-ray imaging during laser melting of Ti-6Al-4V solid metal. The data included here are the time-resolved absolute absorbed power and the Xray images acquired at the same time, along with timing data for synchronization. Also included is information about the experimental configuration including applied laser power, laser beam spatial profile, and the experimental setup. A text document is included that describes all files.

Materials discovery and development necessarily begins with the preparation and identification of product phase(s). Crystalline compounds can be identified by their characteristic diffraction patterns using X-rays, neutrons, and or electrons. An estimated 20,000 X-ray diffractometers and a comparable number of electron microscopes are used daily in materials research and development laboratories for this purpose.

This dataset includes a Microsoft Excel spreadsheet (*.xlsx file) provided as supplemental material for the NIST Technical Note (TN-2099) publication titled "Quasi-Static Position Calibration of the Galvanometer Scanner on the Additive Manufacturing Metrology Testbed". The file contains two tabs, titled "Pre-Compensation" and "Post-Compensation", which provides example measurement data and calculations pertaining to the calibration procedures described in the publication.

Supplementary Data for the paper "Three-Dimensional Particle Shape Analysis Using X-ray Computed Tomography: Experimental Procedure and Analysis Algorithms for Metal Powders" by E.J. Garboczi and N. Hrabe. Contains all the data and programs described in this paper to generate the results discussed in the paper. Also contains all the results that are generated by the data and programs, with which the user can compare to check their results.

This Standard Reference Material (SRM) is intended for use as a primary calibration standard for the quantitative determination of barium. A unit of SRM 3104a consists of five 10 mL sealed borosilicate glass ampoules of an acidified aqueous solution prepared gravimetrically to contain a known mass fraction of barium. The solution contains nitric acid at a volume fraction of approximately 1 %, which is equivalent to a concentration (molarity) of approximately 0.16 mol/L. This data is public in the Certificate of Analysis for this material.

This Standard Reference Material (SRM) is intended for use as a primary calibration standard for the quantitative determination of cerium. A unit of SRM 3110 consists of five 10 mL sealed borosilicate glass ampoules of an acidified aqueous solution prepared gravimetrically to contain a known mass fraction of cerium. The solution contains nitric acid at a mass fraction of approximately 16 %. This data is public in the Certificate of Analysis for this material.